This comprehensive resource delves into various electro-analytical techniques, providing a deep understanding of their principles and applications. Additionally, it covers other vital methods essential for analytical chemistry. Each concept is presented with clarity and precision, ensuring comprehension of even the most intricate topics. With a targeted approach towards exam preparation, this guide meticulously covers the topics most likely to appear in IGNOU exams, facilitating focused revision. From potentiometry to coulometry, each method is elucidated, empowering students to approach exam questions with confidence. Furthermore, practical examples drawn from real-world applications bridge the gap between theory and application, enhancing learning effectiveness. With essential concepts distilled into 50-60 pages, this guide offers a succinct yet comprehensive review, serving as an invaluable resource for last-minute revisions and exam readiness. Master electro-analytical techniques, excel in exams, and pave the path for a successful career in analytical chemistry with our meticulously crafted guide.